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Light Flash Analysis (LFA) employs a shot of light fired into a flat sample to non-destructively determine its thermal diffusivity, heat capacity and thermal conductivity. We use a set of instruments Netzsch LFA 467 and LFA 467 HT to perform measurements in a wide temperature range (200–770 K and 300–1400 K) on disc-shaped samples with a diameter between 6 and 25 mm.